耐火材料 ›› 2022, Vol. 56 ›› Issue (1): 61-64.DOI: 10.3969/j.issn.1001-1935.2022.01.014

• 生产应用 • 上一篇    下一篇

煤气化渣烧结制品的烧成制度研究

牛国峰1)(), 刘芳2,3)(), 贾晓林2,3)   

  1. 1)内蒙古科技大学 理学院 内蒙古包头 014010
    2)内蒙古科技大学 白云鄂博共伴生矿废弃物资源综合利用国家地方联合工程研究中心 内蒙古包头 014010
    3)内蒙古科技大学 白云鄂博矿多金属资源综合利用重点实验室 内蒙古包头 014010
  • 收稿日期:2021-04-01 出版日期:2022-02-15 发布日期:2022-02-24
  • 通讯作者: 刘芳,女,1971年生,硕士,高级工程师。E-mail:liufangbaotou2008@163.com
  • 作者简介:牛国峰:男,1995年生,硕士研究生。E-mail: ngf111@163.com
  • 基金资助:
    内蒙古自治区科技成果转化项目(CGZH2018153)

Research on firing system of coal gasification slag sintered products

Niu Guofeng1)(), Liu Fang2,3)(), Jia Xiaolin2,3)   

  1. 1)College of Sciences,Inner Mongolia University of Science and Technology,Baotou 014010,Inner Mongolia,China
  • Received:2021-04-01 Online:2022-02-15 Published:2022-02-24
  • Contact: Liu Fang

摘要:

以煤气化渣为主要原料制备烧结制品,通过干混料的综合差热分析和样坯的烧成收缩预试验,再根据以往经验,选取升温速率(A)、烧成温度(B)和保温时间(C)三个因素,并分别选取2、3、4 ℃·min -1,1 100、1 150 和1 200 ℃,2、4、6 h为因素水平,选取烧结制品的体积密度、吸水率、耐压强度和热导率为评价指标,按正交表L9(3 3)安排试验。结果表明:1)烧成制度各因素对烧结制品的耐压强度、体积密度和吸水率影响程度的大小顺序均为烧成温度>保温时间>升温速率,对热导率影响程度的大小顺序为烧成温度>升温速率>保温时间。2)经综合平衡考虑,最优试验方案为:升温速率2 ℃·min -1,烧成温度1 200 ℃,保温时间6 h。所得试样的体积密度为1.84 g·cm -3,耐压强度为112 MPa,吸水率为1.44%, 热导率为1.239 W·m -1·K -1

关键词: 煤气化渣, 烧结制品, 正交表, 烧成制度

Abstract:

Sintered products were prepared using coal gasification slag as the main raw material.Based on the comprehensive differential thermal analysis of dry mixture and the firing shrinkage pre-tests of green bodies as well as experience,the experiment was conducted according to orthogonal table L9(3 3),selecting the heating rate,the firing temperature,and the holding time as factors,2,3,and 4 ℃·min -1,1 100,1 150,and 1 200 ℃ as well as 2,4,and 6 h as the corresponding levels,while the bulk density,the water absorption,the compressive strength and the thermal conductivity as evaluation indexes.The results show that:(1)the order of the influence degree of the firing system factors on the compressive strength,the bulk density and the water absorption of the sintered products is the firing temperature>the holding time>the heating rate,and that for the thermal conductivity is the firing temperature>the heating rate>the holding time;(2)generally,the optimal firing system is the heating rate of 2 ℃·min -1,the firing temperature of 1 200 ℃,and the holding time of 6 h,and the prepared sample has the bulk density of 1.84 g·cm -3,the compressive strength of 112 MPa,the water absorption of 1.44%,and the thermal conductivity of 1.239 W·m -1·K -1.

Key words: coal gasification slag, sintered products, orthogonal table, firing system

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